N-(3,4-Difluoro­phen­yl)phthalimide

نویسندگان

  • Xian-Shu Fu
  • Xiao-Ping Yu
  • Wei-Min Wang
  • Fang Lin
چکیده

In the title compound, C(14)H(7)F(2)NO(2), the phthalimide ring system is nearly planar [maximum atomic deviation = 0.028 (1) Å] and it is twisted with respect to the attached benzene ring, making a dihedral angle of 55.70 (6)°. Weak inter-molecular C-H⋯F hydrogen bonds are present in the crystal structure.

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منابع مشابه

ONE STEP SYNTHESIS OF ANILINO ALKYL-NSUBSTITUTED PHTHALIMIDES RELATED TO BENZOISOQUINOLINE-1,3-DIONES (1)

A facile one step synthesis of anilino alky1-N-substituted phthalimide I is reported. The following compounds belonging to this series were made: 1. (anilino-N-ethyl) phthalimide 8 2. (3,4, 5-trimethoxy anilino-N-ethyl) phthalimide 6 3. (3,4, 5-trimethoxy anilino-N-propyl) phthalimide 7 4. N-(ethyl phthalirnido-p-amino benzoyl) glutamic acid diethyl ester 10 5. N-(propyl phthalimido-p-ami...

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N-(3,4-Difluoro­phen­yl)-2-(3,4-dimethoxy­phen­yl)acetamide

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N-(3,4-Difluoro­phen­yl)-3,4-dimethoxy­benzene­sulfonamide

In the title sulfonamide derivative, C(14)H(13)F(2)NO(4)S, the dihedral angle between the benzene rings is 66.05 (9)°. The crystal structure is stabilized by weak inter-molecular N-H⋯O hydrogen bonds involving the amine and meth-oxy groups, which link the mol-ecules into a one-dimensional chain. No significant inter-chain contacts are observed.

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N-(3,4-Difluoro­phen­yl)-N′-(2,5-di­methoxy­phen­yl)urea

In the title compound, C(15)H(14)F(2)N(2)O(3), the dihedral angle between the benzene rings is 64.5 (1)°. One F atom is disordered over two meta positions, with occupancy factors of 0.72 and 0.28. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds involving two N-H and one C=O groups of the urea central fragment, leading to a supra-molecular chain along [011].

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عنوان ژورنال:

دوره 66  شماره 

صفحات  -

تاریخ انتشار 2010